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Rh((C6H5)3PC5H4)(CO)2(1+)*PF6(1-)=Rh((C6H5)3PC5H4)(CO)2PF6

Base Information
  • Chemical Name:Rh((C6H5)3PC5H4)(CO)2(1+)*PF6(1-)=Rh((C6H5)3PC5H4)(CO)2PF6
  • CAS No.:77589-85-6
  • Molecular Formula:C25H19O2PRh*F6P
  • Molecular Weight:630.268
  • Hs Code.:
Rh((C<sub>6</sub>H<sub>5</sub>)3PC<sub>5</sub>H<sub>4</sub>)(CO)2<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Rh((C<sub>6</sub>H<sub>5</sub>)3PC<sub>5</sub>H<sub>4</sub>)(CO)2PF<sub>6</sub>

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Chemical Property of Rh((C6H5)3PC5H4)(CO)2(1+)*PF6(1-)=Rh((C6H5)3PC5H4)(CO)2PF6
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Technology Process of Rh((C6H5)3PC5H4)(CO)2(1+)*PF6(1-)=Rh((C6H5)3PC5H4)(CO)2PF6

There total 1 articles about Rh((C6H5)3PC5H4)(CO)2(1+)*PF6(1-)=Rh((C6H5)3PC5H4)(CO)2PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In acetone; byproducts: AgCl; to stirred acetone soln. of Rh-complex were added solid ligand and AgPF6, after 40 min soln. was filtered at room temp. under N2; solvent was removed by evapn., ppt. was dissolved in CH2Cl2 and Et2O was added; elem. anal.;
Guidance literature:
In dichloromethane; to CH2Cl2 soln. of Rh-complex was added ligand, mixt. was stirred at room temp. for 5 d under N2; Et2O was added, collected, washed with Et2O, dried; elem. anal.;
Guidance literature:
In dichloromethane; to CH2Cl2 soln. of Rh-complex was added ligand, mixt. was stirred at room temp. for 5 d under N2; Et2O was added, collected, washed with Et2O, dried, recrystd. from CH2Cl2-Et2O; elem. anal.;
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