[Re(diethyl ether)(CO)3(2,2'-bipyridyl)]BF₄

Base Information

Chemical Name:[Re(diethyl ether)(CO)3(2,2'-bipyridyl)]BF₄
CAS No.:468083-41-2
Molecular Formula:BF₄*C₁₇H₁₈N₂O₄Re
Molecular Weight:587.353
Hs Code.:

[Re(diethyl ether)(CO)3(2,2'-bipyridyl)]BF<sub>4</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Re(diethyl ether)(CO)3(2,2'-bipyridyl)]BF₄

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Technology Process of [Re(diethyl ether)(CO)3(2,2'-bipyridyl)]BF₄

There total 1 articles about [Re(diethyl ether)(CO)3(2,2'-bipyridyl)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 202349-58-4
[Re(OMe)(CO)3(2,2'-bipyridyl)]

: 468083-41-2
[Re(diethyl ether)(CO)3(2,2'-bipyridyl)]BF₄

: 468083-35-4
[Re(methanol)(CO)3(2,2'-bipyridyl)]B(3,5-bis(trifluoromethyl)phenyl)4

Guidance literature:: In dichloromethane; soln. of Re-contg. compd. (0.109 mmol) in CH2Cl2 was cooled at -78°C; the stoich. amt. of HBF4*Et2O (0.109 mmol) was added; volatiles were removed under vac.; the solid was dissolved in CH2Cl2; slow diffusion of hexanes into this soln. afforded the crystals of the solid; elem. anal.;
DOI:10.1021/ic020174c