2-Chlor-acetophenon-

Base Information

• Chemical Name: 2-Chlor-acetophenon-
• CAS No.: 5757-94-8
• Molecular Formula: C₁₀H₁₃ClN₂
• Molecular Weight: 196.68
• Mol file: 5757-94-8.mol

Synonyms:

Chemical Property of 2-Chlor-acetophenon-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Chlor-acetophenon-

There total 1 articles about 2-Chlor-acetophenon- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-chlorophenyl)ethanone (2142-68-9) + N,N-Dimethylhydrazine (57-14-7) → 2-Chlor-acetophenon- (5757-94-8)

Guidance literature:

In ethanol; Heating;

DOI:10.1021/jo01341a008

Reference yield:

2-Chlor-acetophenon- (5757-94-8) → 2-Chlor-acetophenon-hydrazon (5758-16-7)

Guidance literature:

With hydrazine; In ethanol; Heating;

DOI:10.1021/jo01341a008

Reference yield:

2-Chlor-acetophenon- (5757-94-8) → C13H14Cl2N2 (1448862-53-0)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium diisopropyl amide / tetrahydrofuran / -78 - 0 °C

2: hydrazine hydrate / ethanol / Reflux

With hydrazine hydrate; lithium diisopropyl amide; In tetrahydrofuran; ethanol;

DOI:10.1016/j.bmcl.2013.06.044

upstream raw materials:

1-(2-chlorophenyl)ethanone

N,N-Dimethylhydrazine

Downstream raw materials:

2-Chlor-acetophenon-hydrazon

C₁₃H₁₃ClN₂

C₁₃H₁₄Cl₂N₂