(1-phenyl-3-ethyl-4-methyl-1H-phosphole)heptacarbonyldiiron

Base Information

Chemical Name:(1-phenyl-3-ethyl-4-methyl-1H-phosphole)heptacarbonyldiiron
CAS No.:349586-19-2
Molecular Formula:C₂₀H₁₅Fe₂O₇P
Molecular Weight:510.003
Hs Code.:

Synonyms:

Suppliers and Price of (1-phenyl-3-ethyl-4-methyl-1H-phosphole)heptacarbonyldiiron

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1-phenyl-3-ethyl-4-methyl-1H-phosphole)heptacarbonyldiiron

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1-phenyl-3-ethyl-4-methyl-1H-phosphole)heptacarbonyldiiron

There total 1 articles about (1-phenyl-3-ethyl-4-methyl-1H-phosphole)heptacarbonyldiiron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 64367-52-8
(1-phenyl-3,4-dimethylphosphole)heptacarbonyldiiron

: 74-88-4
methyl iodide

: 349586-19-2
(1-phenyl-3-ethyl-4-methyl-1H-phosphole)heptacarbonyldiiron

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; (N2 or Ar); 1 equiv. lithium diisopropylamide added dropwise to Fe complex/THF at -78°C, stirred for 10 min, MeI added dropwise at -78°C; after 30 min, allowed to warm to room temp.; hydrolysed (satd. soln. of NH4Cl), solvent-removed, extd. (CH2Cl2), washed (H2O), dried (MgSO4), chromd. (SiO2, hexane/toluene); elem. anal.;
DOI:10.1016/S0022-328X(00)00834-2