1,2-bis(oxyacetyl chloride)-4-nitrobenzene

Base Information

Chemical Name:1,2-bis(oxyacetyl chloride)-4-nitrobenzene
CAS No.:78460-93-2
Molecular Formula:C₁₀H₇Cl₂NO₆
Molecular Weight:308.075
Hs Code.:

Synonyms:

Suppliers and Price of 1,2-bis(oxyacetyl chloride)-4-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-bis(oxyacetyl chloride)-4-nitrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-bis(oxyacetyl chloride)-4-nitrobenzene

There total 3 articles about 1,2-bis(oxyacetyl chloride)-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78460-96-5
2,2'-((4-nitro-1,2-phenylene)bis(oxy))diacetic acid

: 78460-93-2
1,2-bis(oxyacetyl chloride)-4-nitrobenzene

Guidance literature:: With thionyl chloride; for 5h; Heating;

Reference yield:

: 3316-09-4
1,2-dihydroxy-4-nitrobenzene

: 78460-93-2
1,2-bis(oxyacetyl chloride)-4-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / anhydrous K₂CO₃ / acetone / Heating; overnight

2: 85 percent / Dowex 50W-x8 (H⁺-form) / H₂O / 8 h / Heating

3: 95 percent / SOCl₂ / 5 h / Heating

With thionyl chloride; potassium carbonate; Dowex 50W-X₈ (H⁺-form); In water; acetone;

Reference yield:

: 78460-95-4
(2-Ethoxycarbonylmethoxy-5-nitro-phenoxy)-acetic acid ethyl ester

: 78460-93-2
1,2-bis(oxyacetyl chloride)-4-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Dowex 50W-x8 (H⁺-form) / H₂O / 8 h / Heating

2: 95 percent / SOCl₂ / 5 h / Heating

With thionyl chloride; Dowex 50W-X₈ (H⁺-form); In water;