C₅₅H₉₂NO₁₀P

Base Information

Chemical Name:C₅₅H₉₂NO₁₀P
CAS No.:1246747-06-7
Molecular Formula:C₅₅H₉₂NO₁₀P
Molecular Weight:958.31
Hs Code.:

C<sub>55</sub>H<sub>92</sub>NO<sub>10</sub>P

Synonyms:

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Chemical Property of C₅₅H₉₂NO₁₀P

Chemical Property:

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Technology Process of C₅₅H₉₂NO₁₀P

There total 11 articles about C₅₅H₉₂NO₁₀P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 883878-93-1
(2S,10R)-3-hydroxy-2-(palmitoyloxy)propyl 10-methyloctadecanoate

: 162406-70-4
[2-(benzyloxy-diisopropylamino-phosphanyloxy)-ethyl]-carbamic acid benzyl ester

: 1246747-06-7
C₅₅H₉₂NO₁₀P

Guidance literature:: (2S,10R)-3-hydroxy-2-(palmitoyloxy)propyl 10-methyloctadecanoate; [2-(benzyloxy-diisopropylamino-phosphanyloxy)-ethyl]-carbamic acid benzyl ester; With 4,5-dicyano-1H-imidazole; In dichloromethane; at 0 ℃; Schlenk technique;

With tert.-butylhydroperoxide; In decane; dichloromethane; at -20 ℃; Schlenk technique;
DOI:10.1039/c3ob41483c

Reference yield:

: (R)-10-methyloctadec-7-enoic acid

: 1246747-06-7
C₅₅H₉₂NO₁₀P

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrazine hydrate; riboflavin / 24 h / 21 °C / Inert atmosphere; Schlenk technique

2.1: [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II) / diethyl ether / 0.25 h / 21 °C / Inert atmosphere; Schlenk technique

2.2: 0.08 h / Inert atmosphere; Schlenk technique

2.3: 16 h / Inert atmosphere; Schlenk technique

3.1: dicyclohexyl-carbodiimide; dmap / n-heptane / 16 h / 0 °C / Schlenk technique

4.1: acetonitrile boron trifluoride complex / dichloromethane / 0.08 h / 21 °C / Schlenk technique

5.1: 4,5-dicyano-1H-imidazole / dichloromethane / 0 °C / Schlenk technique

5.2: -20 °C / Schlenk technique

With dmap; 4,5-dicyano-1H-imidazole; [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); acetonitrile boron trifluoride complex; hydrazine hydrate; dicyclohexyl-carbodiimide; riboflavin; In diethyl ether; n-heptane; dichloromethane;
DOI:10.1039/c3ob41483c

Reference yield:

: 124-19-6
nonan-1-al

: 1246747-06-7
C₅₅H₉₂NO₁₀P

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium chloride / water / 21 °C / Schlenk technique

2.1: copper(I) bromide dimethylsulfide complex / diethyl ether; tert-butyl methyl ether / 0.17 h / -78 °C / Schlenk technique

2.2: 19 h / Schlenk technique

3.1: diisobutylaluminium hydride / dichloromethane / 2 h / Schlenk technique; Cooling with ethanol-dry ice

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 21 °C / Schlenk technique

4.2: 3 h / Schlenk technique

5.1: hydrazine hydrate; riboflavin / 24 h / 21 °C / Inert atmosphere; Schlenk technique

6.1: [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II) / diethyl ether / 0.25 h / 21 °C / Inert atmosphere; Schlenk technique

6.2: 0.08 h / Inert atmosphere; Schlenk technique

6.3: 16 h / Inert atmosphere; Schlenk technique

7.1: dicyclohexyl-carbodiimide; dmap / n-heptane / 16 h / 0 °C / Schlenk technique

8.1: acetonitrile boron trifluoride complex / dichloromethane / 0.08 h / 21 °C / Schlenk technique

9.1: 4,5-dicyano-1H-imidazole / dichloromethane / 0 °C / Schlenk technique

9.2: -20 °C / Schlenk technique

With dmap; 4,5-dicyano-1H-imidazole; [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); copper(I) bromide dimethylsulfide complex; acetonitrile boron trifluoride complex; diisobutylaluminium hydride; hydrazine hydrate; dicyclohexyl-carbodiimide; lithium chloride; lithium hexamethyldisilazane; riboflavin; In tetrahydrofuran; diethyl ether; n-heptane; dichloromethane; tert-butyl methyl ether; water; 1.1: |Wittig Olefination / 4.2: |Wittig Olefination;
DOI:10.1039/c3ob41483c