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Technology Process of Os(ClC6H4NCHC6H2CH3OH)(P(C6H5)3)2Br(CO)2

Os(ClC6H4NCHC6H2CH3OH)(P(C6H5)3)2Br(CO)2

Base Information
  • Chemical Name:Os(ClC6H4NCHC6H2CH3OH)(P(C6H5)3)2Br(CO)2
  • CAS No.:861659-64-5
  • Molecular Formula:C52H41BrClNO3OsP2
  • Molecular Weight:1095.41
  • Hs Code.:
Os(ClC<sub>6</sub>H<sub>4</sub>NCHC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>OH)(P(C<sub>6</sub>H<sub>5</sub>)3)2Br(CO)2

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Chemical Property of Os(ClC6H4NCHC6H2CH3OH)(P(C6H5)3)2Br(CO)2
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Technology Process of Os(ClC6H4NCHC6H2CH3OH)(P(C6H5)3)2Br(CO)2

There total 1 articles about Os(ClC6H4NCHC6H2CH3OH)(P(C6H5)3)2Br(CO)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

Os(ClC<sub>6</sub>H<sub>4</sub>NHCHC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>O)(P(C<sub>6</sub>H<sub>5</sub>)3)2Cl(CO)

Os(ClC6H4NHCHC6H2CH3O)(P(C6H5)3)2Cl(CO)

carbon monoxide
201230-82-2

carbon monoxide

Os(ClC<sub>6</sub>H<sub>4</sub>NCHC<sub>6</sub>H<sub>2</sub>CH<sub>3</sub>OH)(P(C<sub>6</sub>H<sub>5</sub>)3)2Br(CO)2
861659-64-5

Os(ClC6H4NCHC6H2CH3OH)(P(C6H5)3)2Br(CO)2

Guidance literature:
In dichloromethane; N2 was passed through a soln. of complex in CH2Cl2 for 15 min followed by CO (1 atm) for 10 min, the soln. was left under CO atm for 6 h with constant stirring; evapd. under reduced pressure, dissolved in min CH2Cl2, petroleum ether was added, crystals were dried in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2005.04.012
upstream raw materials:

carbon monoxide

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