C₁₆H₁₀N₄O₂S

Base Information

Chemical Name:C₁₆H₁₀N₄O₂S
CAS No.:1204771-96-9
Molecular Formula:C₁₆H₁₀N₄O₂S
Molecular Weight:322.347
Hs Code.:

C<sub>16</sub>H<sub>10</sub>N<sub>4</sub>O<sub>2</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₀N₄O₂S

Chemical Property:

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Technology Process of C₁₆H₁₀N₄O₂S

There total 7 articles about C₁₆H₁₀N₄O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1569279-57-7
C₁₈H₁₄N₄O₂S

: 1204771-96-9
C₁₆H₁₀N₄O₂S

Guidance literature:: With sodium hydroxide; In ethanol; at 20 ℃;
DOI:10.1016/j.bmcl.2014.01.052

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1204771-96-9
C₁₆H₁₀N₄O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 0 - 20 °C

2: Dess-Martin periodane / dichloromethane / 20 °C

3: hydrazine hydrate / ethanol / Reflux

4: (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide; potassium phosphate; 1,3,5-trimethyl-benzene / 185 °C

5: sodium hydroxide / ethanol / 20 °C

With potassium phosphate; copper(l) iodide; (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; Dess-Martin periodane; hydrazine hydrate; sodium hydroxide; 1,3,5-trimethyl-benzene; In tetrahydrofuran; ethanol; dichloromethane; 4: |Buchwald Indole Synthesis;
DOI:10.1016/j.bmcl.2014.01.052

Reference yield:

: 1519354-49-4
C₁₂H₈FNO

: 1204771-96-9
C₁₆H₁₀N₄O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / Reflux

2: (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide; potassium phosphate; 1,3,5-trimethyl-benzene / 185 °C

3: sodium hydroxide / ethanol / 20 °C

With potassium phosphate; copper(l) iodide; (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; hydrazine hydrate; sodium hydroxide; 1,3,5-trimethyl-benzene; In ethanol; 2: |Buchwald Indole Synthesis;
DOI:10.1016/j.bmcl.2014.01.052