Technology Process of C28H20F6O4
There total 5 articles about C28H20F6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfuric acid; acetic acid; periodic acid / 5 h / 70 °C
2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane
3: tetrabutylammomium bromide; rongalite / N,N-dimethyl-formamide / 6 h / 0 - 20 °C
4: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; XPhos / tetrahydrofuran; water; toluene / 15 h / 60 °C / Inert atmosphere
5: toluene / 30 h / Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); N-Bromosuccinimide; sulfuric acid; tetrabutylammomium bromide; rongalite; sodium carbonate; acetic acid; periodic acid; XPhos; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide; toluene;
4: Suzuki-Miyaura cross-coupling reaction / 5: Diels-Alder reaction;
DOI:10.3987/COM-10-S(E)63
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutylammomium bromide; rongalite / N,N-dimethyl-formamide / 6 h / 0 - 20 °C
2: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; XPhos / tetrahydrofuran; water; toluene / 15 h / 60 °C / Inert atmosphere
3: toluene / 30 h / Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); tetrabutylammomium bromide; rongalite; sodium carbonate; XPhos;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
2: Suzuki-Miyaura cross-coupling reaction / 3: Diels-Alder reaction;
DOI:10.3987/COM-10-S(E)63