1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

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Chemical Name:1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione
CAS No.:1191934-05-0
Molecular Formula:C₄₄H₃₈N₄O₈
Molecular Weight:750.808
Hs Code.:

1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

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Chemical Property of 1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

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Technology Process of 1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

There total 2 articles about 1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: C₂₆H₂₄I₂N₄O₆

: 1191934-03-8
C₂₆H₂₄I₂N₄O₆

: 768-60-5
4-methoxyphenylacetylen

: 1,8-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

: 1191934-05-0
1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 12h; Inert atmosphere;
DOI:10.3184/030823409X439717

Reference yield:

: 1191934-06-1
1,2-dibromo-3-iodobenzene

: 161146-03-8
1,5-bis(carboxyethyl)glycoluril

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 768-60-5
4-methoxyphenylacetylen

: 1,8-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

: 1191934-05-0
1,11-di(4-methoxyphenylethynyl)-13b,13c-diethoxycarbonyl-6H,13H-5,7,12,13b,13c,14-hexahydro-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

Guidance literature:: 1,5-bis(carboxyethyl)glycoluril; dimethyl sulfoxide; With potassium tert-butylate; at 20 ℃; for 0.216667h; Inert atmosphere;

1,2-dibromo-3-iodobenzene; In dimethyl sulfoxide; at 20 ℃; for 3h; Inert atmosphere;

4-methoxyphenylacetylen; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 12h; Inert atmosphere;
DOI:10.3184/030823409X439717