Technology Process of C56H66N14O12
There total 5 articles about C56H66N14O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / CH2Cl2 / 0.08 h / 0 °C
2: 75 percent / 40percent HBr/HOAc / 0.25 h / 23 °C
3: 1. LiOH 2. dicyclohexylcarbodimide, N-hydroxybenzotriazole / 1. THF, H2O 2. DMF
With
lithium hydroxide; hydrogen bromide; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide;
In
dichloromethane;
DOI:10.1021/jo00302a033
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dicyclohexylcarbodiimide
2: 93 percent / CH2Cl2 / 0.08 h / 0 °C
3: 75 percent / 40percent HBr/HOAc / 0.25 h / 23 °C
4: 1. LiOH 2. dicyclohexylcarbodimide, N-hydroxybenzotriazole / 1. THF, H2O 2. DMF
With
lithium hydroxide; hydrogen bromide; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide;
In
dichloromethane;
DOI:10.1021/jo00302a033
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 75 percent / 40percent HBr/HOAc / 0.25 h / 23 °C
2: 1. LiOH 2. dicyclohexylcarbodimide, N-hydroxybenzotriazole / 1. THF, H2O 2. DMF
With
lithium hydroxide; hydrogen bromide; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide;
DOI:10.1021/jo00302a033