salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone

Base Information

Chemical Name:salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone
CAS No.:68096-02-6
Molecular Formula:C₂₃H₁₇N₃O₂
Molecular Weight:367.407
Hs Code.:

Synonyms:

Suppliers and Price of salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone

There total 2 articles about salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4779-54-8
2-phenylquinoline-4-carboxylic acid hydrazide

: 90-02-8
salicylaldehyde

: 68096-02-6
salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone

Guidance literature:: for 3h; Reflux;
DOI:10.1016/j.inoche.2011.06.005

Reference yield:

: 68096-02-6
salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone

Guidance literature:: Hydrazid 1b, entspr. Carbonylverb.;
DOI:10.1002/ardp.19783110906

Reference yield:

: 6018-89-9
nickel(II) acetate tetrahydrate

: 68096-02-6
salicylaldehyde 2-phenylquinoline-4-carbonylhydrazone

: [(OC₆H₄CHNNCOC₉H₅NC₆H₅)Ni]2*[(OC₆H₄CHNNCOC₉H₅NC₆H₅)Ni(H₂O)2]2*4H₂O

Guidance literature:: With NaOH; In ethanol; ligand and NaOH (1:1) mixed, stirred for 0.5 h, treated with Ni(OAc)2*4H2O (1.25 equiv.), stirred at room temp. for 3 h; pptd.(H2O), filtered, washed (C2H5OH/H2O 1:1), dried (vac.), elem. anal.;
DOI:10.1016/j.inoche.2011.06.005