O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α,β-D-glucopyranosylamine

Base Information

Chemical Name:O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α,β-D-glucopyranosylamine
CAS No.:131088-77-2
Molecular Formula:C₆₁H₈₁N₃O₂₈
Molecular Weight:1304.32
Hs Code.:

O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N-<N-(tert-butoxycarbonyl)-L-aspart-1-oyl-(L-proline methyl ester)-4-oyl>-α,β-D-glucopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α,β-D-glucopyranosylamine

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Technology Process of O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α,β-D-glucopyranosylamine

There total 16 articles about O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α,β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.1%

: 131088-76-1
N-(tert-butoxycarbonyl)-L-aspartyl-L-proline methyl ester

: 138850-57-4,138850-58-5
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α,β-D-glucopyranosyl amine

: 131088-77-2,131176-19-7
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α,β-D-glucopyranosylamine

Guidance literature:: With diethyl cyanophosphonate;
DOI:10.1248/cpb.40.296

Reference yield: 62.0%

: 131088-75-0,131176-18-6
2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

: 81129-75-1
2,3,4,2',3',4',6'-hepta-O-acetyl-α-D-isomaltosyl bromide

: 131088-77-2,131176-19-7
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; In nitromethane; at 55 ℃; for 6h;
DOI:10.1016/0008-6215(90)80006-O

Reference yield: 40.0%

: 131088-75-0,131176-18-6
2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

: 81129-75-1
2,3,4,2',3',4',6'-hepta-O-acetyl-α-D-isomaltosyl bromide

: 131088-77-2,131176-19-7
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; tetramethylurea; In nitromethane; -14 deg C, 2 h then r.t. for 6 h;
DOI:10.1016/0008-6215(90)80006-O