[Nd(pentaethylene glycol)(picrato)2](picrate)

Base Information

• Chemical Name: [Nd(pentaethylene glycol)(picrato)2](picrate)
• CAS No.: 1192036-49-9
• Molecular Formula: C₆H₂N₃O₇*C₂₂H₂₆N₆NdO₂₀
• Molecular Weight: 1066.81
• Mol file: 1192036-49-9.mol

Synonyms:

Chemical Property of [Nd(pentaethylene glycol)(picrato)2](picrate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Nd(pentaethylene glycol)(picrato)2](picrate)

There total 1 articles about [Nd(pentaethylene glycol)(picrato)2](picrate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Pentaethylene glycol (4792-15-8) + neodymium(III) nitrate pentahydrate + 2,4,6-Trinitrophenol (88-89-1) → [Nd(pentaethylene glycol)(picrato)2](picrate) (1192036-49-9)

Guidance literature:

In methanol; acetonitrile; slow addn. of pentaethylene glycol and Nd(NO3)3*5H2O to picric acid soln. into mixt. NeCN:MeOH (3:1, v/v) at room temp. under stirring for 5 min; slow evapn. at room temp., crystn. for 1-5 days; elem. anal.;

DOI:10.1016/j.saa.2009.05.024

Reference yield:

[Nd(pentaethylene glycol)(picrato)2](picrate) (1192036-49-9) + dimethyl sulfoxide (67-68-5,8070-53-9) → [Nd(pentaethylene glycol)(DMSO)3](picrate)3

Guidance literature:

In dimethyl sulfoxide; dissolving in DMSO;

DOI:10.1016/j.saa.2009.05.024

upstream raw materials:

Pentaethylene glycol

2,4,6-Trinitrophenol