2-hydroxyacetophenone nicotinic acid hydrazone

Base Information

Chemical Name:2-hydroxyacetophenone nicotinic acid hydrazone
CAS No.:74734-33-1
Molecular Formula:C₁₄H₁₃N₃O₂
Molecular Weight:255.276
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxyacetophenone nicotinic acid hydrazone

Chemical Property:

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Technology Process of 2-hydroxyacetophenone nicotinic acid hydrazone

There total 1 articles about 2-hydroxyacetophenone nicotinic acid hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1452-63-7
picolinic acid hydrazide

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 74734-33-1
2-hydroxyacetophenone nicotinic acid hydrazone

Guidance literature:: With ethanol;
DOI:10.1021/ja01117a519

Reference yield:

: 74734-33-1
o-hydroxyacetophenone 2-picoloyl hydrazone

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: Co⁽²⁺⁾*2C₅H₄NCONHNC(CH₃)C₆H₄OH*2Cl^(1-)*H₂O = [Co(C₅H₄NCONHNC(CH₃)C₆H₄OH)2]Cl₂*H₂O

Guidance literature:: In methanol; ethanol; acetone; soln. of the org. compd. in acetone/alcohol (1:1) treated with a soln. of the metal salt in MeOH, refluxed for 1 h; filtered, washed with MeOH, air dried, elem. anal.;
DOI:10.1016/0022-1902(81)80437-X

Reference yield:

: 74734-33-1
o-hydroxyacetophenone 2-picoloyl hydrazone

: 83864-14-6
nickel dichloride

: Ni⁽²⁺⁾*2C₅H₄NCONHNC(CH₃)C₆H₄OH*2Cl^(1-)*H₂O = [Ni(C₅H₄NCONHNC(CH₃)C₆H₄OH)2]Cl₂*H₂O

Guidance literature:: In methanol; ethanol; acetone; soln. of the org. compd. in acetone/alcohol (1:1) treated with a soln. of the metal salt in MeOH, refluxed for 1 h; filtered, washed with MeOH, air dried, elem. anal.;
DOI:10.1016/0022-1902(81)80437-X