p-nitrophenyl 5-oxo-3-phenylpentanoate

Base Information

Chemical Name:p-nitrophenyl 5-oxo-3-phenylpentanoate
CAS No.:131906-21-3
Molecular Formula:C₁₇H₁₅NO₅
Molecular Weight:313.31
Hs Code.:

Synonyms:

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Chemical Property of p-nitrophenyl 5-oxo-3-phenylpentanoate

Chemical Property:

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Technology Process of p-nitrophenyl 5-oxo-3-phenylpentanoate

There total 4 articles about p-nitrophenyl 5-oxo-3-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132015-40-8
3-phenyl-pentanedioic acid monomethyl ester

: 131906-21-3
p-nitrophenyl 5-oxo-3-phenylpentanoate

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / BH₃*SMe₂ / tetrahydrofuran; diethyl ether / 1.5 h / Heating

2: 86 percent / pyridinium chlorochromate / CH₂Cl₂ / 0.42 h / Heating

3: 90 percent / toluenesulfonic acid / benzene / 5.5 h / Heating

4: 82 percent / 5percent KOH / methanol / 2 h

5: 57 percent / toluenesulfonic acid, H₂O / acetone / 48 h / Heating

6: DCC / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, 30 min

With potassium hydroxide; dimethylsulfide borane complex; o-toluenesulfonic acid; water; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone; benzene;
DOI:10.1021/jm00107a041

Reference yield:

: 132015-42-0
methyl 5-oxo-3-phenylpentanoate

: 131906-21-3
p-nitrophenyl 5-oxo-3-phenylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / toluenesulfonic acid / benzene / 5.5 h / Heating

2: 82 percent / 5percent KOH / methanol / 2 h

3: 57 percent / toluenesulfonic acid, H₂O / acetone / 48 h / Heating

4: DCC / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, 30 min

With potassium hydroxide; o-toluenesulfonic acid; water; dicyclohexyl-carbodiimide; In methanol; dichloromethane; acetone; benzene;
DOI:10.1021/jm00107a041

Reference yield:

: 131906-17-7
methyl 5-hydroxy-3-phenylpentanoate

: 131906-21-3
p-nitrophenyl 5-oxo-3-phenylpentanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / pyridinium chlorochromate / CH₂Cl₂ / 0.42 h / Heating

2: 90 percent / toluenesulfonic acid / benzene / 5.5 h / Heating

3: 82 percent / 5percent KOH / methanol / 2 h

4: 57 percent / toluenesulfonic acid, H₂O / acetone / 48 h / Heating

5: DCC / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, 30 min

With potassium hydroxide; o-toluenesulfonic acid; water; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In methanol; dichloromethane; acetone; benzene;
DOI:10.1021/jm00107a041