4-nitro-benzoic acid-[4]phenanthrylamide

Base Information

• Chemical Name: 4-nitro-benzoic acid-[4]phenanthrylamide
• CAS No.: 855263-19-3
• Molecular Formula: C₂₁H₁₄N₂O₃
• Molecular Weight: 342.354
• Mol file: 855263-19-3.mol

Synonyms:

Chemical Property of 4-nitro-benzoic acid-[4]phenanthrylamide

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-nitro-benzoic acid-[4]phenanthrylamide

There total 1 articles about 4-nitro-benzoic acid-[4]phenanthrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-phenanthrenamine (17423-48-2) + 4-nitro-benzoyl chloride (122-04-3) → 4-nitro-benzoic acid-[4]phenanthrylamide (855263-19-3)

Guidance literature:

DOI:10.1039/jr9510002487

Reference yield:

4-nitro-benzoic acid-[4]phenanthrylamide (855263-19-3) → 5-(4-nitro-phenyl)-benzo[lmn]phenanthridine (860709-95-1)

Guidance literature:

With nitrobenzene; trichlorophosphate; at 160 ℃;

DOI:10.1039/jr9510002487

Reference yield:

4-nitro-benzoic acid-[4]phenanthrylamide (855263-19-3) → 5-(4-amino-phenyl)-4-methyl-benzo[lmn]phenanthridinium; toluene-4-sulfonate

Guidance literature:

Multi-step reaction with 2 steps

1: phosphoryl chloride; nitrobenzene / 160 °C

2: nitrobenzene; iron-powder; aq.-ethanolic HCl

With hydrogenchloride; iron; nitrobenzene; trichlorophosphate;

DOI:10.1039/jr9510002487

upstream raw materials:

4-phenanthrenamine

4-nitro-benzoyl chloride

Downstream raw materials:

5-(4-nitro-phenyl)-benzo[lmn]phenanthridine