C₃₉H₂₆S

Base Information

Chemical Name:C₃₉H₂₆S
CAS No.:1384864-45-2
Molecular Formula:C₃₉H₂₆S
Molecular Weight:526.701
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₂₆S

Chemical Property:

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Technology Process of C₃₉H₂₆S

There total 8 articles about C₃₉H₂₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1384864-44-1
1,4-diphenyl-2,3-bis(bromomethyl)-9,9'-spirobifluorene

: 1384864-45-2
C₃₉H₂₆S

Guidance literature:: With sodiumsulfide nonahydrate; In tetrahydrofuran; ethanol; for 3h; Inert atmosphere; Reflux;
DOI:10.3987/COM-12-12427

Reference yield:

: 1384864-32-7
3,3-dimethyl-6,12-diphenyl-1H-fluoreno[2,3-e][1,3]dioxepin-11(5H)-one

: 1384864-45-2
C₃₉H₂₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: formic acid / 24 h / Reflux

3.1: potassium hydroxide / tetrahydrofuran; water / 0.5 h

4.1: sulfuric acid; tetrabutylammomium bromide; hydrogen bromide / chloroform; water / 72 h / 60 °C

5.1: sodiumsulfide nonahydrate / tetrahydrofuran; ethanol / 3 h / Inert atmosphere; Reflux

With n-butyllithium; formic acid; sodiumsulfide nonahydrate; sulfuric acid; tetrabutylammomium bromide; hydrogen bromide; potassium hydroxide; In tetrahydrofuran; ethanol; hexane; chloroform; water;
DOI:10.3987/COM-12-12427

Reference yield:

: 6583-74-0
1,3-diphenylcyclopenta[a]indene-2,8-dione

: 1384864-45-2
C₃₉H₂₆S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 0.08 h / 240 °C

2.1: toluene-4-sulfonic acid / tetrahydrofuran / 4 h / Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

3.2: 2 h / -78 - 20 °C / Inert atmosphere

4.1: formic acid / 24 h / Reflux

5.1: potassium hydroxide / tetrahydrofuran; water / 0.5 h

6.1: sulfuric acid; tetrabutylammomium bromide; hydrogen bromide / chloroform; water / 72 h / 60 °C

7.1: sodiumsulfide nonahydrate / tetrahydrofuran; ethanol / 3 h / Inert atmosphere; Reflux

With n-butyllithium; formic acid; sodiumsulfide nonahydrate; sulfuric acid; tetrabutylammomium bromide; hydrogen bromide; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; ethanol; hexane; chloroform; water; 1.1: Diels-Alder reaction;
DOI:10.3987/COM-12-12427