5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one

Base Information

Chemical Name:5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one
CAS No.:87379-34-8
Molecular Formula:C₁₉H₁₅N₃O
Molecular Weight:301.348
Hs Code.:

5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d><l>benzazepin-6(6H)-one

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Chemical Property of 5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one

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Technology Process of 5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one

There total 4 articles about 5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 2217-79-0
diphenyliodonium iodide

: 87379-33-7
2-methyl-5,7-dihydropyrimido<5,4-d>-benzazepin-6(6H)-one

: 87379-34-8
5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one

Guidance literature:: With sodium methylate; copper(l) chloride; In methanol; for 3h; Heating;
DOI:10.1002/jhet.5570200330

Reference yield:

: 4424-80-0
2,3,4,5-tetrahydro-1H-1-benzo[b]azepin-2-one

: 87379-34-8
5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: 26 percent / potassium permanganate, magnesium nitrate hexahydrate / 2-methyl-propan-2-ol; H₂O / 20 h / Ambient temperature

2: 87 percent / 1 h / 115 - 120 °C

3: 83 percent / sodium methoxide / methanol / 2.5 h / Ambient temperature

4: 56 percent / cuprous chloride, sodium methoxide / methanol / 3 h / Heating

With magnesium(II) nitrate; potassium permanganate; sodium methylate; copper(l) chloride; In methanol; water; tert-butyl alcohol;
DOI:10.1002/jhet.5570200330

Reference yield:

: 16511-38-9
1H-[1]benzazepin-2,5(3H,4H)-dione

: 87379-34-8
5,7-dihydro-2-methyl-7-phenylpyrimido<5,4-d>benzazepin-6(6H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 1 h / 115 - 120 °C

2: 83 percent / sodium methoxide / methanol / 2.5 h / Ambient temperature

3: 56 percent / cuprous chloride, sodium methoxide / methanol / 3 h / Heating

With sodium methylate; copper(l) chloride; In methanol;
DOI:10.1002/jhet.5570200330