tetrakis(2-ethoxyphenyl)bismuthonium ftoluene-p-sulfonate

Base Information

Chemical Name:tetrakis(2-ethoxyphenyl)bismuthonium ftoluene-p-sulfonate
CAS No.:193489-97-3
Molecular Formula:C₇H₇O₃S*C₃₂H₃₆BiO₄
Molecular Weight:864.813
Hs Code.:

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Chemical Property of tetrakis(2-ethoxyphenyl)bismuthonium ftoluene-p-sulfonate

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Technology Process of tetrakis(2-ethoxyphenyl)bismuthonium ftoluene-p-sulfonate

There total 2 articles about tetrakis(2-ethoxyphenyl)bismuthonium ftoluene-p-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: tetrakis(2-ethoxyphenyl)bismuthonium chloride monohydrate

: 657-84-1
sodium tosylate

: 193489-97-3
tetrakis(2-ethoxyphenyl)bismuthonium ftoluene-p-sulfonate

Guidance literature:: In chloroform; water; aq. Na-salt soln. addn. to Bi-salt soln. (CHCl3), mixt. stirring vigorously 2 h at room temp., org. layer sepn., aq. layer extn. (CHCl3); combined org. extracts evapn., chromy. (silica gel, CH2Cl2/EtOH 1:0 to 10:1); elem. anal.;
DOI:10.1039/a700379j

Reference yield:

: 157731-20-9
tris(2-ethoxyphenyl)bismuthane

: 193489-97-3
tetrakis(2-ethoxyphenyl)bismuthonium ftoluene-p-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: iodosylbenzene / chloroform

2: water; chloroform

With iodosylbenzene; In chloroform; water;
DOI:10.1039/a700379j