Technology Process of C39H66O18
There total 3 articles about C39H66O18 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 76 percent / dibenzo-18-crown-6, BaO, Ba(OH)2*8H2O / dimethylformamide / 1.) -8 deg C (ice-salt bath), 2.) room temp., 16 h
2: dicobalt octacarbonyl / dioxane / 115.2 h / Heating
With
barium dihydroxide; dibenzo-18-crown-6; barium(II) oxide;
dicobalt octacarbonyl;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jo00146a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 56 percent / SnCl4 / 1,2-dichloro-ethane / 4 h / Ambient temperature
2: 76 percent / dibenzo-18-crown-6, BaO, Ba(OH)2*8H2O / dimethylformamide / 1.) -8 deg C (ice-salt bath), 2.) room temp., 16 h
3: dicobalt octacarbonyl / dioxane / 115.2 h / Heating
With
barium dihydroxide; dibenzo-18-crown-6; tin(IV) chloride; barium(II) oxide;
dicobalt octacarbonyl;
In
1,4-dioxane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00146a023
- Guidance literature:
-
dicobalt octacarbonyl;
In
1,4-dioxane;
for 115.2h;
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
Heating;
DOI:10.1021/jo00146a023