Methanesulfonic acid (R)-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester

Base Information

Chemical Name:Methanesulfonic acid (R)-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester
CAS No.:71748-65-7
Molecular Formula:C₁₄H₂₆O₁₀S₂
Molecular Weight:418.486
Hs Code.:

Methanesulfonic acid (R)-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester

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Chemical Property of Methanesulfonic acid (R)-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester

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Technology Process of Methanesulfonic acid (R)-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester

There total 1 articles about Methanesulfonic acid (R)-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7115-24-4,71748-65-7,117859-45-7,127707-50-0
2,3;5,6-Di-O-isopropyliden-1,4-di-O-methansulfonyl-galactit

Guidance literature:: aus 2,3;5,6-Di-O-isopropyliden-galactit in Py., Methansulfonylchlorid;
DOI:10.1039/jr9610003656

Reference yield:

: 71748-65-7
Methanesulfonic acid (R)-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-((4R,5S)-5-methanesulfonyloxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester

: 24578-06-1
1,4-dideoxy-1,4-imino-D-glucitol

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / sodium azide / dimethylformamide; H₂O / 4 h / Heating

2: 74 percent / trifluoroacetic acid / methanol; H₂O / 1 h / 100 °C

3: 3.1 g / pyridine / Ambient temperature

4: 1.) 0.6 M barium methoxide, 2.) formic acid, conc. ammonia / 2.) 10 percent Pd/C / 1.) methanol, rt, 30 min, 2.) methanol, heating

With ammonium hydroxide; formic acid; sodium azide; barium methoxide; trifluoroacetic acid; palladium on activated charcoal; In pyridine; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90194-0