C₂₇H₂₆Cl₂N₂O₆S

Base Information

• Chemical Name: C₂₇H₂₆Cl₂N₂O₆S
• CAS No.: 1612849-03-2
• Molecular Formula: C₂₇H₂₆Cl₂N₂O₆S
• Molecular Weight: 577.485
• Mol file: 1612849-03-2.mol

Synonyms:

Chemical Property of C₂₇H₂₆Cl₂N₂O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₂₆Cl₂N₂O₆S

There total 6 articles about C₂₇H₂₆Cl₂N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H30Cl2N2O6S (1622236-20-7) → C27H26Cl2N2O6S (1612849-03-2)

Guidance literature:

With water; lithium hydroxide; In methanol; at 20 ℃;

DOI:10.1016/j.bmcl.2014.04.092

Reference yield:

4-methyl-2-pentanone (108-10-1) → C27H26Cl2N2O6S (1612849-03-2)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium tert-butylate / dimethyl sulfoxide / 20 °C

2: sulfuric acid

3: tin(ll) chloride / ethyl acetate / Reflux

4: pyridine / 20 °C

5: lithium hydroxide; water / methanol / 20 °C

With pyridine; sulfuric acid; potassium tert-butylate; water; tin(ll) chloride; lithium hydroxide; In methanol; dimethyl sulfoxide; ethyl acetate;

DOI:10.1016/j.bmcl.2014.04.092

Reference yield:

2-(4-(4-amino-2-nitrophenoxy)-3-methoxyphenyl)acetic acid (1080521-35-2) → C27H26Cl2N2O6S (1612849-03-2)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium tert-butylate / dimethyl sulfoxide / 20 °C

2: sulfuric acid

3: tin(ll) chloride / ethyl acetate / Reflux

4: pyridine / 20 °C

5: lithium hydroxide; water / methanol / 20 °C

With pyridine; sulfuric acid; potassium tert-butylate; water; tin(ll) chloride; lithium hydroxide; In methanol; dimethyl sulfoxide; ethyl acetate;

DOI:10.1016/j.bmcl.2014.04.092

upstream raw materials:

4-methyl-2-pentanone

2-(4-(4-amino-2-nitrophenoxy)-3-methoxyphenyl)acetic acid

C₂₁H₂₂N₂O₆

C₂₃H₂₈N₂O₄