Phenazine,5,10-diacetyl-5,10-dihydro- (6CI,8CI,9CI)

Base Information

• Chemical Name: Phenazine,5,10-diacetyl-5,10-dihydro- (6CI,8CI,9CI)
• CAS No.: 7478-17-3
• Molecular Formula: C16H14 N2 O2
• Molecular Weight: 266.299
• Mol file: 7478-17-3.mol

Synonyms:9,10-Diacetyl-9,10-dihydrophenazine;NSC 402879

Chemical Property of Phenazine,5,10-diacetyl-5,10-dihydro- (6CI,8CI,9CI)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenazine,5,10-diacetyl-5,10-dihydro- (6CI,8CI,9CI)

There total 3 articles about Phenazine,5,10-diacetyl-5,10-dihydro- (6CI,8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,10-dihydrophenazine (613-32-1) + acetic anhydride (108-24-7) → 5-acetyl-5,10-dihydrophenazine (18345-95-4) + 1,1′-(phenazin-5,10-diyl)diethanone (7478-17-3)

Guidance literature:

at 135 ℃; for 0.166667h; Overall yield = 75 %; Overall yield = 600 mg;

Reference yield:

Phenazin (92-82-0) → 5-acetyl-5,10-dihydrophenazine (18345-95-4) + 1,1′-(phenazin-5,10-diyl)diethanone (7478-17-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydrogen sulfate / water; ethanol / Reflux

2: 0.17 h / 135 °C

With sodium hydrogen sulfate; In ethanol; water;

Reference yield:

5-acetyl-5,10-dihydrophenazine (18345-95-4) + acetic anhydride (108-24-7) → 1,1′-(phenazin-5,10-diyl)diethanone (7478-17-3)

Guidance literature:

upstream raw materials:

5-acetyl-5,10-dihydrophenazine

acetic anhydride

5,10-dihydrophenazine

Phenazin

Downstream raw materials:

2-chlorophenazine