2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate

Base Information

Chemical Name:2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate
CAS No.:1344992-53-5
Molecular Formula:C₂₄H₂₁ClF₄N₂O₈
Molecular Weight:576.886
Hs Code.:

2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate

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Chemical Property of 2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate

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Technology Process of 2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate

There total 8 articles about 2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 344420-23-1
2,5-difluoro-4-[3-methyl-2,6-dioxo-4-(trifluoromethyl)-1,2,3,6-tetrahydropyrimidin-1-yl]nitrobenzene

: 1344992-53-5
2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 70 °C

2: acetic acid; iron / water / 2 h / 35 °C

3: copper(l) chloride; copper dichloride; isopentyl nitrite / acetonitrile / 1 h / 20 °C

4: boron tribromide / dichloromethane / 48 h / 20 °C

5: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 20 - 60 °C / Inert atmosphere

6: indium(III) chloride / 9 h / 75 - 82 °C

7: sodium 4-methylbenzenesulfinate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; methanol / 6 h / 20 °C

8: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 20 °C

With indium(III) chloride; boron tribromide; iron; potassium carbonate; acetic acid; sodium 4-methylbenzenesulfinate; N-ethyl-N,N-diisopropylamine; copper(l) chloride; copper dichloride; isopentyl nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 497866-29-2
3-[2-chloro-4-fluoro-5-(3-methyl-2,6-dioxo-4-trifluoromethyl-1,2,3,6-tetrahydropyrimidin-1-yl)phenoxy]-2-methoxypyridine

: 1344992-53-5
2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate

Guidance literature:: Multi-step reaction with 5 steps

1: boron tribromide / dichloromethane / 48 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 20 - 60 °C / Inert atmosphere

3: indium(III) chloride / 9 h / 75 - 82 °C

4: sodium 4-methylbenzenesulfinate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; methanol / 6 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 20 °C

With indium(III) chloride; boron tribromide; potassium carbonate; sodium 4-methylbenzenesulfinate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 497866-09-8
3-(4-chloro-2-fluoro-5-((2-oxo-1,2-dihydropyridin-3-yl)oxy)phenyl)-1-methyl-6-(trifluoromethyl)pyrimidine-2,4(1H,3H)-dione

: 1344992-53-5
2-methoxyethyl 2-[2-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]phenoxy]-2-methoxyacetate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 20 - 60 °C / Inert atmosphere

2: indium(III) chloride / 9 h / 75 - 82 °C

3: sodium 4-methylbenzenesulfinate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; methanol / 6 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 20 °C

With indium(III) chloride; potassium carbonate; sodium 4-methylbenzenesulfinate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;