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Technology Process of C32H44O5Si

C32H44O5Si

Base Information
  • Chemical Name:C32H44O5Si
  • CAS No.:1352816-36-4
  • Molecular Formula:C32H44O5Si
  • Molecular Weight:536.784
  • Hs Code.:
C<sub>32</sub>H<sub>44</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C32H44O5Si
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Technology Process of C32H44O5Si

There total 1 articles about C32H44O5Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C<sub>32</sub>H<sub>46</sub>O<sub>6</sub>Si
1352816-02-4

C32H46O6Si

C<sub>32</sub>H<sub>44</sub>O<sub>5</sub>Si
1352816-36-4

C32H44O5Si

Guidance literature:
With toluene-4-sulfonic acid; sodium sulfate; In acetone; at 50 ℃; for 1h;
DOI:10.1002/anie.201104681

Reference yield:

C<sub>32</sub>H<sub>44</sub>O<sub>5</sub>Si
1352816-36-4

C32H44O5Si

benzoyl chloride
98-88-4

benzoyl chloride

C<sub>39</sub>H<sub>48</sub>O<sub>6</sub>Si

C39H48O6Si

Guidance literature:
With pyridine; dmap; In dichloromethane; at 20 ℃; for 17h; Inert atmosphere;
DOI:10.1002/anie.201104681

Reference yield:

C<sub>32</sub>H<sub>44</sub>O<sub>5</sub>Si
1352816-36-4

C32H44O5Si

C<sub>47</sub>H<sub>60</sub>O<sub>8</sub>Si
1352816-05-7

C47H60O8Si

Guidance literature:
Multi-step reaction with 2 steps
1.1: pyridine; dmap / dichloromethane / 17 h / 20 °C / Inert atmosphere
2.1: potassium hexamethylsilazane / tetrahydrofuran / 1 h / -40 - -20 °C
2.2: 0.08 h / -20 °C
2.3: 0.83 h / -20 - 0 °C
With pyridine; dmap; potassium hexamethylsilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201104681
upstream raw materials:

C32H46O6Si

Downstream raw materials:

C47H60O8Si

C47H60O8Si

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