[Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)

Base Information

Chemical Name:[Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)
CAS No.:569648-96-0
Molecular Formula:C₈₆H₁₁₈Mo₂N₈
Molecular Weight:1455.82
Hs Code.:

Synonyms:

Suppliers and Price of [Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)

There total 1 articles about [Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.3%

: Mo(N[((t)Bu)(3,5-C₆H₃Me₂)])3

: 100-47-0
benzonitrile

: 569648-96-0
[Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)

Guidance literature:: In diethyl ether; under N2 atm. using Schlenk techniques; to soln. of Mo complex in Et2O added PhCN; mixed at 20°C; solvent evapd. to dryness for 72 h; extd. and crystd. from cold toluene;elem. anal.;
DOI:10.1021/om030124v

Reference yield:

: 569648-96-0
[Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)

: 256240-25-2
NMo(N[((t)Bu)(3,5-C₆H₃Me₂)])3

Guidance literature:: In ⁽²⁾H₈-toluene; neither at room temp. nor upon extended heating (2 h at 100°C);
DOI:10.1021/om030124v

Reference yield:

: 569648-96-0
[Mo(N[t-Bu][3,5-C6H3Me2])3]2(μ-NCPhCPhN)

: [Mo(N[t-Bu][3,5-C6H3Me2])2(N-3,5-C6H3Me2)]2(μ-NCPhCPhN)

Guidance literature:: In toluene; byproducts: isobutene, isobutylene, hexamethylethane; under N2 atm. using Schlenk techniques; soln. of Mo complex in toluene thermolyzed in 105°C oil bath for 1.5 h; monitored by NMR; elem. anal.;
DOI:10.1021/om030124v