tributyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate

Base Information

Chemical Name:tributyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate
CAS No.:460745-54-4
Molecular Formula:C₂₆H₃₈O₃SSn
Molecular Weight:549.362
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Chemical Property of tributyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate

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Technology Process of tributyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate

There total 2 articles about tributyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.75%

: 460745-63-5
silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid

: 1461-22-9
tributyltin chloride

: 460745-54-4
tributyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate

Guidance literature:: In chloroform; byproducts: AgCl; (C4H9)3SnCl (CHCl3) added dropwise with stirring to suspn. of silver salt of 5-benzoyl-α-methyl-2-thiophene acetic acid (CHCl3); refluxed for 7-8 h under He; stand overnight at 25°C; AgCl filtered; solvent removed under reduced pressure; recrystd. (CH2Cl2/n-hexane 1:1); elem. anal.;
DOI:10.1081/SIM-120004439

Reference yield:

: 33005-95-7
tiaprofenic acid

: 460745-54-4
tributyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / water; ethanol

2: chloroform

With NaHCO₃; In ethanol; chloroform; water;
DOI:10.1081/SIM-120004439