silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid

Base Information

Chemical Name:silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid
CAS No.:460745-63-5
Molecular Formula:Ag*C₁₄H₁₁O₃S
Molecular Weight:367.174
Hs Code.:

Synonyms:

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Chemical Property of silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid

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Technology Process of silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid

There total 1 articles about silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33005-95-7
tiaprofenic acid

: silver nitrate

: 460745-63-5
silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid

Guidance literature:: With NaHCO₃; In ethanol; water; soln. of acid ligand, soln. NaHCO3 added dropwise with stirring; soln. AgNO3 added dropwise; ppt.; mixt. stirred for 15 min;; filtered through Buechner; solid washed twice (C2H5OH);
DOI:10.1081/SIM-120004439

Reference yield: 82.8%

: 460745-63-5
silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid

: 683-18-1
dibutyltin chloride

: 460745-53-3
dibutyl-bis(5-benzoyl-α-methyl-2-thiopheneacetate)tin(IV)

Guidance literature:: In chloroform; byproducts: AgCl; (C4H9)2SnCl2 (CHCl3) added dropwise with stirring to suspn. of silver salt of 5-benzoyl-α-methyl-2-thiophene acetic acid (CHCl3); refluxedfor 7-8 h under He; stand overnight at 25°C; AgCl filtered; solvent removed under reduced pressure; recrystd. (CH2Cl2/n-hexane 1:1); elem. anal.;
DOI:10.1081/SIM-120004439

Reference yield: 79.0%

: 460745-63-5
silver salt of 5-benzoyl-α-methyl-2-thiopheneaceticacid

: 1066-45-1
trimethyltin(IV)chloride

: 460745-56-6
trimethyltin(IV) 5-benzoyl-α-methyl-2-thiophene acetate

Guidance literature:: In chloroform; byproducts: AgCl; (CH3)3SnCl (CHCl3) added dropwise with stirring to suspn. of silver saltof 5-benzoyl-α-methyl-2-thiophene acetic acid (CHCl3); refluxed f or 7-8 h under He; stand overnight at 25°C; AgCl filtered; solvent removed under reduced pressure; recrystd. (CH2Cl2/n-hexane 1:1); elem. anal.;
DOI:10.1081/SIM-120004439