N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure

Base Information

Chemical Name:N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure
CAS No.:127027-87-6
Molecular Formula:C₁₆H₁₆ClNO₄
Molecular Weight:321.76
Hs Code.:

Synonyms:

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Chemical Property of N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure

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Technology Process of N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure

There total 5 articles about N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16766-30-6
4-Chloroguaiacol

: 127027-87-6
N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / 100 percent HNO₃, AcOH / 1 h / 10 °C

2: 98 percent / K₂CO₃, Ki / dimethylformamide / 4 h / 80 °C

3: hydrogen, conc. NH₄OH / 5 percent Pd/C / dimethylsulfoxide; tetrahydrofuran / 15 °C

4: NaHCO₃ / tetrahydrofuran; H₂O / 1.5 h / 0 °C

With ammonium hydroxide; hydrogen; nitric acid; sodium hydrogencarbonate; potassium carbonate; acetic acid; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19890720717

Reference yield:

: 90-05-1
2-methoxy-phenol

: 127027-87-6
N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / SO₂Cl₂ / CHCl₃ / 35 °C

2: 41 percent / 100 percent HNO₃, AcOH / 1 h / 10 °C

3: 98 percent / K₂CO₃, Ki / dimethylformamide / 4 h / 80 °C

4: hydrogen, conc. NH₄OH / 5 percent Pd/C / dimethylsulfoxide; tetrahydrofuran / 15 °C

5: NaHCO₃ / tetrahydrofuran; H₂O / 1.5 h / 0 °C

With ammonium hydroxide; sulfuryl dichloride; hydrogen; nitric acid; sodium hydrogencarbonate; potassium carbonate; acetic acid; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19890720717

Reference yield:

: 127027-86-5
2-(Benzyloxy)-4-chloro-2-methoxy-6-nitrobenzol

: 127027-87-6
N-<2-(Benzyloxy)-5-chloro-3-methoxyphenyl>acetohydroxamsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen, conc. NH₄OH / 5 percent Pd/C / dimethylsulfoxide; tetrahydrofuran / 15 °C

2: NaHCO₃ / tetrahydrofuran; H₂O / 1.5 h / 0 °C

With ammonium hydroxide; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1002/hlca.19890720717