2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid

Base Information

Chemical Name:2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid
CAS No.:1397694-82-4
Molecular Formula:C₇₆H₈₂N₄O₄S₂
Molecular Weight:1179.64
Hs Code.:

2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid

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Chemical Property of 2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid

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Technology Process of 2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid

There total 6 articles about 2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1397694-85-7
5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophene-2-carbaldehyde

: 372-09-8
cyanoacetic acid

: 1397694-82-4
2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid

Guidance literature:: With piperidine; In tetrahydrofuran; acetonitrile; for 8h; Reflux;
DOI:10.1039/c2jm33833e

Reference yield:

: 1190978-95-0
3,6-dibromo-4,5-bis(hexyloxy)benzene-1,2-diamine

: 1397694-82-4
2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: toluene / 6 h / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 12 h / Inert atmosphere; Reflux

3: trichlorophosphate / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

4: N-Bromosuccinimide / chloroform / 10 h / 20 °C / Darkness

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 24 h / 80 °C / Inert atmosphere

6: piperidine / tetrahydrofuran; acetonitrile / 8 h / Reflux

With piperidine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trichlorophosphate; In tetrahydrofuran; chloroform; water; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1039/c2jm33833e

Reference yield:

: 1397694-78-8
11,12-bis(hexyloxy)-10,13-bis(4-hexylthiophen-2-yl)dibenzo[a,c]phenazine

: 1397694-82-4
2-cyano-3-(5-(13-(5-(4-(dip-tolylamino)phenyl)-4-hexylthiophen-2-yl)-11,12-bis(hexyloxy)dibenzo[a,c]phenazin-10-yl)-3-hexylthiophen-2-yl)acrylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

2: N-Bromosuccinimide / chloroform / 10 h / 20 °C / Darkness

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 24 h / 80 °C / Inert atmosphere

4: piperidine / tetrahydrofuran; acetonitrile / 8 h / Reflux

With piperidine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trichlorophosphate; In tetrahydrofuran; chloroform; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/c2jm33833e