C₃₃H₂₆F₃N₅O₈S

Base Information

• Chemical Name: C₃₃H₂₆F₃N₅O₈S
• CAS No.: 118149-20-5
• Molecular Formula: C₃₃H₂₆F₃N₅O₈S
• Molecular Weight: 709.659
• Mol file: 118149-20-5.mol

Synonyms:

Chemical Property of C₃₃H₂₆F₃N₅O₈S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₂₆F₃N₅O₈S

There total 4 articles about C₃₃H₂₆F₃N₅O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trifluoromethane sulfonyl chloride (421-83-0) + C32H27N5O6 (118149-17-0) → C33H26F3N5O8S (118149-20-5)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 ℃;

DOI:10.1039/c39880000898

Reference yield:

benzoyl chloride (98-88-4) → C33H26F3N5O8S (118149-20-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) pyridine, 2.) NH₃ / 2.) MeOH

2: 72 percent / potassium t-butoxide / tetrahydrofuran / -35 °C

3: NEt₃, 4-dimethylaminopyridine / CH₂Cl₂ / 0 °C

With pyridine; dmap; potassium tert-butylate; ammonia; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c39880000898

Reference yield:

aristeromycin (19186-33-5) → C33H26F3N5O8S (118149-20-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) pyridine, 2.) NH₃ / 2.) MeOH

2: 72 percent / potassium t-butoxide / tetrahydrofuran / -35 °C

3: NEt₃, 4-dimethylaminopyridine / CH₂Cl₂ / 0 °C

With pyridine; dmap; potassium tert-butylate; ammonia; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c39880000898

upstream raw materials:

trifluoromethane sulfonyl chloride

C₃₂H₂₇N₅O₆

benzoyl chloride

aristeromycin

Downstream raw materials:

C₃₂H₂₆FN₅O₅

Refernces