(S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester

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Chemical Name:(S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester
CAS No.:91682-52-9
Molecular Formula:C₄₈H₆₆N₈O₁₀S
Molecular Weight:947.166
Hs Code.:

(S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester

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Chemical Property of (S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester

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Technology Process of (S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester

There total 9 articles about (S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 45233-75-8
2-[[(2S)-2-(tert-butoxycarbonylamino)-3-methyl-butanoyl]amino]acetic acid

: 91682-52-9
(S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 67 percent / HOBt, 1-ethyl-3,3-dimethylaminopropylcarbodiimide / H₂O

2: TFA,

3: 82.5 percent / TEA,

4: TFA,

5: 85 percent / TEA,

6: TFA,

7: 74.6 percent / NMM,

8: TFA,

With 4-methyl-morpholine; TEA; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; In water;
DOI:10.1246/cl.1984.1013

Reference yield:

: 16217-56-4
(S,S)-leucinylmethionine amide

: 91682-52-9
(S)-3-Amino-N-((S)-2-benzyloxy-1-{(S)-1-[(S)-1-({[(S)-1-((S)-1-carbamoyl-3-methylsulfanyl-propylcarbamoyl)-3-methyl-butylcarbamoyl]-methyl}-carbamoyl)-2-methyl-propylcarbamoyl]-2-phenyl-ethylcarbamoyl}-ethyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 67 percent / HOBt, 1-ethyl-3,3-dimethylaminopropylcarbodiimide / H₂O

2: TFA,

3: 82.5 percent / TEA,

4: TFA,

5: 85 percent / TEA,

6: TFA,

7: 74.6 percent / NMM,

8: TFA,

With 4-methyl-morpholine; TEA; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; In water;
DOI:10.1246/cl.1984.1013