Technology Process of C28H23F2NO3
There total 8 articles about C28H23F2NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid; zinc / 70 °C
2: (bis-(2-methoxyethyl)amino)sulfur trufluoride / ethanol; dichloromethane
3: palladium on activated charcoal; hydrogen / ethanol
4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide
With
palladium on activated charcoal; hydrogen; potassium carbonate; acetic acid; potassium iodide; (bis-(2-methoxyethyl)amino)sulfur trufluoride; zinc;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.064
- Guidance literature:
-
Multi-step reaction with 5 steps
1: Zn-Cu couple / 1,2-dimethoxyethane; diethyl ether / 50 °C
2: acetic acid; zinc / 70 °C
3: (bis-(2-methoxyethyl)amino)sulfur trufluoride / ethanol; dichloromethane
4: palladium on activated charcoal; hydrogen / ethanol
5: potassium carbonate; potassium iodide / N,N-dimethyl-formamide
With
palladium on activated charcoal; hydrogen; potassium carbonate; acetic acid; potassium iodide; (bis-(2-methoxyethyl)amino)sulfur trufluoride; zinc;
In
1,2-dimethoxyethane; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.064
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / ethanol; dichloromethane
2: palladium on activated charcoal; hydrogen / ethanol
3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide
With
palladium on activated charcoal; hydrogen; potassium carbonate; potassium iodide; (bis-(2-methoxyethyl)amino)sulfur trufluoride;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.064