tris(phenylethynyl)stibane

Base Information

Chemical Name:tris(phenylethynyl)stibane
CAS No.:37003-05-7
Molecular Formula:C₂₄H₁₅Sb
Molecular Weight:425.133
Hs Code.:
Mol file:37003-05-7.mol

Synonyms:NSC 248851

Suppliers and Price of tris(phenylethynyl)stibane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of tris(phenylethynyl)stibane

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tris(phenylethynyl)stibane

There total 4 articles about tris(phenylethynyl)stibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 6738-06-3
phenylethynylmagnesium bromide

: 10025-91-9
antimony(III) chloride

: 37003-05-7
Triphenylaethinyl-antimon

Guidance literature:: With aq. NH₄Cl; In tetrahydrofuran; dropwise addn. of soln. of SbCl3 in THF to cold soln. of stoich. amt. of BrMgCCPh in THF (-15°C, under N2), allowed to warm up, stirred (20°C, 2 h), hydrolysis with 10% aq. NH4Cl (-10°C), extn. with ether; ext. washed with satd. NaCl-soln., dried with Na2SO4, evapn. of solvent in high vac.;