methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate

Base Information

Chemical Name:methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate
CAS No.:79414-49-6
Molecular Formula:C₂₄H₂₉NO₁₂S₂
Molecular Weight:587.626
Hs Code.:

methyl <O(1)-benzyl-2-C-(benzyloxy)formamido>-2-deoxy-3,4-bis<O(methylsulfonyl)>-α-D-glucopyranosiduronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate

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Technology Process of methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate

There total 1 articles about methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79414-48-5
methyl -2-deoxy-α-D-glucopyranosiduronate

: 124-63-0
methanesulfonyl chloride

: 79414-49-6
methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate

Guidance literature:: With pyridine;
DOI:10.1002/hlca.19810640535

Reference yield: 100.0%

: 79414-49-6
methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate

: 687-47-8
(S)-Ethyl lactate

: (5R,6S)-6-Benzyloxy-5-benzyloxycarbonylamino-2-((S)-1-ethoxycarbonyl-ethoxy)-5,6-dihydro-2H-pyran-2-carboxylic acid methyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; Ambient temperature;
DOI:10.1002/hlca.19810640535

Reference yield:

: 79414-49-6
methyl -2-deoxy-3,4-bis-α-D-glucopyranosiduronate

: ((2S,3R)-2-Benzyloxy-6-carbamoyl-6-methoxy-3,6-dihydro-2H-pyran-3-yl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / Ambient temperature

2: NH₃ / methanol

With potassium hydroxide; ammonia; In methanol;
DOI:10.1002/hlca.19810640535