Methyl 3-aMino-4,5-dichlorobenzoate

Base Information

• Chemical Name: Methyl 3-aMino-4,5-dichlorobenzoate
• CAS No.: 1250663-38-7
• Molecular Formula: C₈H₇Cl₂NO₂
• Molecular Weight: 220.055
• Mol file: 1250663-38-7.mol

Synonyms:

Chemical Property of Methyl 3-aMino-4,5-dichlorobenzoate

Chemical Property:

• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

99%, ^*data from raw suppliers

methyl3-amino-4,5-dichlorobenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 3-aMino-4,5-dichlorobenzoate

There total 3 articles about Methyl 3-aMino-4,5-dichlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3,4-dichloro-5-nitrobenzoate (63105-53-3) → C8H7Cl2NO2 (1250663-38-7)

Guidance literature:

With iron; ammonium chloride; In water; at 80 ℃; for 1h;

Reference yield:

3,4-dichlorbenzoic acid (51-44-5) → C8H7Cl2NO2 (1250663-38-7)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride / 12 h / 0 - 70 °C

2: nitric acid; sulfuric acid / 1.2 h / 0 °C

3: iron; ammonium chloride / water / 1 h / 80 °C

With thionyl chloride; sulfuric acid; nitric acid; iron; ammonium chloride; In water;

Reference yield:

methyl 3,4-dichlorobenzoate (2905-68-2) → C8H7Cl2NO2 (1250663-38-7)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid; sulfuric acid / 1.2 h / 0 °C

2: iron; ammonium chloride / water / 1 h / 80 °C

With sulfuric acid; nitric acid; iron; ammonium chloride; In water;

upstream raw materials:

3,4-dichlorbenzoic acid

methyl 3,4-dichlorobenzoate

methyl 3,4-dichloro-5-nitrobenzoate

Refernces