Technology Process of C33H46N4O7
There total 8 articles about C33H46N4O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1021/jm301630s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen; palladium on activated charcoal / ethyl acetate / 2 h / 760.05 Torr
2: methanol / 3 h / 0 - 20 °C
3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
4: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 0 - 20 °C
With
1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm301630s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen; palladium on activated charcoal / ethyl acetate / 2 h / 760.05 Torr
2: potassium carbonate / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 20 °C / Cooling with ice
3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
4: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 0 - 20 °C
With
1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm301630s
