C₂₄H₂₅⁽²⁾HN₂O₅

Base Information

Chemical Name:C₂₄H₂₅⁽²⁾HN₂O₅
CAS No.:203510-17-2
Molecular Formula:C₂₄H₂₆N₂O₅
Molecular Weight:423.473
Hs Code.:

C<sub>24</sub>H<sub>25</sub><sup>(2)</sup>HN<sub>2</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₅⁽²⁾HN₂O₅

Chemical Property:

Purity/Quality:

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Technology Process of C₂₄H₂₅⁽²⁾HN₂O₅

There total 8 articles about C₂₄H₂₅⁽²⁾HN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34311-63-2
5-O-benzyl-3-oxo-1,2-O-isopropylidene-α-D-xylofuranose

: 203510-17-2
C₂₄H₂₅⁽²⁾HN₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: NaB⁽²⁾H₄ / ethanol

2: NaH / dimethylformamide

3: TsOH / dioxane; H₂O

4: pyridine; acetonitrile

5: 88 percent / bis(trimethylsilylacetamide), SnCl₄ / acetonitrile

6: 85 percent / NH₃ / methanol

7: 1.) phenyl chlorothionoformate, DMAP; 2.) Bu₃SnH, AIBN / 1.) CH₂Cl₂; 2.) benzene, reflux

With dmap; sodium borodeuteride; bis(trimethylsilylacetamide); 2,2'-azobis(isobutyronitrile); ammonia; tri-n-butyl-tin hydride; tin(IV) chloride; sodium hydride; toluene-4-sulfonic acid; phenylcarbonochloridothioate; In 1,4-dioxane; pyridine; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(97)10815-2

Reference yield:

: 20031-21-4
1,2-O-isopropylidene-α-D-xylose

: 203510-17-2
C₂₄H₂₅⁽²⁾HN₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) (Bu₃Sn)2O; 2.) Bu₄NI; 3.) triacetoxy periodinane / 1.) toluene; 2.) toluene

2: NaB⁽²⁾H₄ / ethanol

3: NaH / dimethylformamide

4: TsOH / dioxane; H₂O

5: pyridine; acetonitrile

6: 88 percent / bis(trimethylsilylacetamide), SnCl₄ / acetonitrile

7: 85 percent / NH₃ / methanol

8: 1.) phenyl chlorothionoformate, DMAP; 2.) Bu₃SnH, AIBN / 1.) CH₂Cl₂; 2.) benzene, reflux

With dmap; sodium borodeuteride; bis(trimethylsilylacetamide); 2,2'-azobis(isobutyronitrile); ammonia; tri-n-butyl-tin hydride; tin(IV) chloride; tetra-(n-butyl)ammonium iodide; sodium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; bis(tri-n-butyltin)oxide; phenylcarbonochloridothioate; In 1,4-dioxane; pyridine; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(97)10815-2

Reference yield:

: C₁₅H₁₈⁽²⁾H₂O₅

: 203510-17-2
C₂₄H₂₅⁽²⁾HN₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1: NaH / dimethylformamide

2: TsOH / dioxane; H₂O

3: pyridine; acetonitrile

4: 88 percent / bis(trimethylsilylacetamide), SnCl₄ / acetonitrile

5: 85 percent / NH₃ / methanol

6: 1.) phenyl chlorothionoformate, DMAP; 2.) Bu₃SnH, AIBN / 1.) CH₂Cl₂; 2.) benzene, reflux

With dmap; bis(trimethylsilylacetamide); 2,2'-azobis(isobutyronitrile); ammonia; tri-n-butyl-tin hydride; tin(IV) chloride; sodium hydride; toluene-4-sulfonic acid; phenylcarbonochloridothioate; In 1,4-dioxane; pyridine; methanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(97)10815-2