(2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol

Base Information

Chemical Name:(2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol
CAS No.:126451-10-3
Molecular Formula:C₂₈H₄₆O₈
Molecular Weight:510.668
Hs Code.:

(2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol

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Chemical Property of (2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol

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Technology Process of (2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol

There total 3 articles about (2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 126365-80-8
(2S,3R,6R)-6-<(2S,5RS)-5-<(R)-1-2-hydroxy-1-(4-methoxybenzyloxy)ethyl>-5-methoxy-2-methyltetrahydrofuran-2-yl>-3-ethyl-2-methyltetrahydropyran-3-ol

: 77-76-9
2,2-dimethoxy-propane

: 126451-10-3
(2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol

Guidance literature:: With camphor-10-sulfonic acid; for 0.25h; Ambient temperature;
DOI:10.1248/cpb.37.1726

Reference yield:

: 126365-78-4
(2S,3R,6R)-6-<(2S,5RS)-5-<(R)-1-2-acetoxy-1-(4-methoxybenzyloxy)ethyl>-5-hydroxy-2-methyltetrahydrofuran-2-yl>-3-ethyl-2-methyltetrahydropyran-3-ol

: 126451-10-3
(2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / CSA / 0.25 h / Ambient temperature

2: 100 percent / KOH / H₂O / 0.33 h / Ambient temperature

3: 96 percent / CSA / 0.25 h / Ambient temperature

With potassium hydroxide; camphor-10-sulfonic acid; In water;
DOI:10.1248/cpb.37.1726

Reference yield:

: 126365-79-5
Acetic acid (R)-2-[(S)-5-((2R,5R,6S)-5-ethyl-5-hydroxy-6-methyl-tetrahydro-pyran-2-yl)-2-methoxy-5-methyl-tetrahydro-furan-2-yl]-2-(4-methoxy-benzyloxy)-ethyl ester

: 126451-10-3
(2S,3R,6R)-3-Ethyl-6-{(S)-5-methoxy-5-[(R)-1-(4-methoxy-benzyloxy)-2-(1-methoxy-1-methyl-ethoxy)-ethyl]-2-methyl-tetrahydro-furan-2-yl}-2-methyl-tetrahydro-pyran-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / KOH / H₂O / 0.33 h / Ambient temperature

2: 96 percent / CSA / 0.25 h / Ambient temperature

With potassium hydroxide; camphor-10-sulfonic acid; In water;
DOI:10.1248/cpb.37.1726