nickel(II) dimandelate

Base Information

• Chemical Name: nickel(II) dimandelate
• CAS No.: 37134-87-5
• Molecular Formula: 2C₈H₇O₃*Ni
• Molecular Weight: 360.974
• Mol file: 37134-87-5.mol

Synonyms:

Chemical Property of nickel(II) dimandelate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of nickel(II) dimandelate

There total 3 articles about nickel(II) dimandelate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

nickel(II) chloride hexahydrate + (R)-Mandelic Acid (611-71-2) → nickel(II) dimandelate (19944-55-9,37134-87-5)

Guidance literature:

With NaOH; In water; High Pressure; metal:acid:NaOH:water=2:4:4:20 molar ratio, homogenised, heated in bomb at 170°C for 120 h; ppt. washed (water, abs. ethanol); elem. anal.;

DOI:10.1002/ejic.200400623

Reference yield:

sodium DL-mandelate (114-21-6) + nickel dichloride (83864-14-6) → nickel(II) dimandelate (19944-55-9,37134-87-5)

Guidance literature:

In water; soln. of sodium mandelate added to aq. soln. of metal salt; mixt. heatedfor about 1 h; ppt. filtered off; washed (H2O purged with N2); dried at ambient temp.; kept in desiccator (anhyd. CaCl2); elem. anal.;

DOI:10.1016/j.tca.2012.01.012

Reference yield:

→ nickel(II) dimandelate (19944-55-9,37134-87-5)

Guidance literature:

Mandelsaeure, Ni(ClO4)2;

upstream raw materials:

(R)-Mandelic Acid

sodium DL-mandelate

nickel dichloride

Downstream raw materials:

nickel(II) oxide