10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Base Information

Chemical Name:10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin
CAS No.:302897-08-1
Molecular Formula:C₄₃H₄₉N₅O₁₇
Molecular Weight:907.885
Hs Code.:

10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Synonyms:

Suppliers and Price of 10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

There total 5 articles about 10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 67670-69-3
N-acetyl-4,7,8,9-tetra-O-acetyl-2-chloro-2-deoxyneuraminic acid methyl ester

: 302897-04-7
10-(6-hydroxy-hexyl)-6-nitro-3-phenyl-10H-pyrimido[4,5-b]quinoline-2,4-dione

: 302897-00-3
10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-β-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

: 302897-08-1
10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Guidance literature:: With 4 Angstroem MS; silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/S0968-0896(00)00124-3

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 302897-08-1
10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / butan-1-ol / 3 h / Heating

2: 72 percent / dimethylformamide / 3 h / 120 °C

3: 20 percent / 4 Angstroem MS; AgOTf / CH₂Cl₂ / 1 h / 20 °C

With 4 Angstroem MS; silver trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide; butan-1-ol; 1: Substitution / 2: Cyclization / 3: Substitution;
DOI:10.1016/S0968-0896(00)00124-3

Reference yield:

: 1644-82-2
2-fluoro-6-nitrobenzaldehyde

: 302897-08-1
10-[6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosylonate)hexyl]-6-nitro-3-phenyl-5-deazaflavin

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / dimethylformamide / 3 h / 120 °C

2: 20 percent / 4 Angstroem MS; AgOTf / CH₂Cl₂ / 1 h / 20 °C

With 4 Angstroem MS; silver trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide; 1: Cyclization / 2: Substitution;
DOI:10.1016/S0968-0896(00)00124-3