[Ni(CH₂SiMe₃)2(PMe₂Ph)2]

Base Information

Chemical Name:[Ni(CH₂SiMe₃)2(PMe₂Ph)2]
CAS No.:78054-44-1
Molecular Formula:C₂₄H₄₄NiP₂Si₂
Molecular Weight:509.422
Hs Code.:

[Ni(CH<sub>2</sub>SiMe<sub>3</sub>)2(PMe<sub>2</sub>Ph)2]

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Chemical Property of [Ni(CH₂SiMe₃)2(PMe₂Ph)2]

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Technology Process of [Ni(CH₂SiMe₃)2(PMe₂Ph)2]

There total 2 articles about [Ni(CH₂SiMe₃)2(PMe₂Ph)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14076-99-4,20154-73-8,36829-43-3
[nickel(II)(pyridine)4(chloride)2]

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: 672-66-2
Dimethyl(phenyl)phosphine

: 78054-44-1
[Ni(CH₂SiMe₃)2(PMe₂Ph)2]

Guidance literature:: With pyridine; In pyridine; diethyl ether; under oxygen-fre nitrogen, Mg(CH2SiMe3)Cl in diethyl ether syringed onto mixture of NiCl2(py)4, pyridine, PMe2Ph, diethyl ether with stirring at -60°C, suspension warmed to 25°C and stirred for 1 h; evapn. to dryness to vac., extn. with light petroleum, centrifugation, partial removal of solvent, cooling at -30°C, elem. anal.;
DOI:10.1039/DT9810000777

Reference yield: 80.0%

: cis-Ni(CH₂SiMe₃)2py2

: 672-66-2
Dimethyl(phenyl)phosphine

: 78054-44-1
[Ni(CH₂SiMe₃)2(PMe₂Ph)2]

Guidance literature:: In light petroleum; under oxygen-free nitrogen, stirred for 4-5 min at 0°C under oxygen-free nitrogen, colour changed from red to yellow; solvent removed in vac., residue dissolved in light petroleum, centrifuged, crystd. from light petroleum at -30°C, elem. anal.;
DOI:10.1039/DT9810000777