sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane

Base Information

Chemical Name:sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane
CAS No.:261908-91-2
Molecular Formula:C₂₀H₃₄N₃O₂*Na
Molecular Weight:371.499
Hs Code.:

Synonyms:

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Chemical Property of sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane

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Technology Process of sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane

There total 1 articles about sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 121-00-6,1341-82-8
3-tert-Butyl-4-hydroxyanisole

: 1,4-dimethyl-1,4,7-triazacyclononane

: 261908-91-2
sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1021/ja970417d

Reference yield: 58.0%

: 22658-72-6
potassium 1,3-dioxo-1,3-diphenylpropan-2-ide

: cobalt(II) perchlorate hexahydrate

: 261908-91-2
sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane

: [Co((CH₃NCH₂CH₂)2(CH₂)2NCH₂(C₆H₂)O(OCH₃)(C₄H₉))(C₆H₅C(O)CHC(O)C₆H₅)]⁽¹⁺⁾*ClO₄^(1-)=[C₃₅H₄₅CoN₃O₄](ClO₄)

Guidance literature:: In methanol; cobalt salt mixed with tetradentate ligand in methanol and refluxed under argon for 1 h; cooled, K(Ph2acac) added; crystn. on storage at ambient temp. for 2 h, filtration; elem. anal.;
DOI:10.1016/S0020-1693(99)00314-X

Reference yield: 53.0%

: gallium(III) perchlorate hexahydrate

: 22658-72-6
potassium 1,3-dioxo-1,3-diphenylpropan-2-ide

: 261908-91-2
sodium 1,4-dimethyl-7-(3-tert-butyl-5-methoxy-2-hydroxybenzyl)-1,4,7-triazacyclononane

: [Ga((CH₃NCH₂CH₂)2(CH₂)2NCH₂(C₆H₂)O(OCH₃)(C₄H₉))(C₆H₅C(O)CHC(O)C₆H₅)]⁽¹⁺⁾*ClO₄^(1-)=[C₃₅H₄₅GaN₃O₄](ClO₄)

Guidance literature:: In methanol; soln. of tetradentate ligand and metal salt refluxed in methanol for 1 h, K(Ph2acac) added; pptn., filtration, recrystn. from CH3CN/CH2Cl2 (1:1); elem. anal.;
DOI:10.1016/S0020-1693(99)00314-X