C₂₅H₂₄N₆O₃

Base Information

Chemical Name:C₂₅H₂₄N₆O₃
CAS No.:701213-67-4
Molecular Formula:C₂₅H₂₄N₆O₃
Molecular Weight:456.504
Hs Code.:

C<sub>25</sub>H<sub>24</sub>N<sub>6</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₅H₂₄N₆O₃

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Technology Process of C₂₅H₂₄N₆O₃

There total 5 articles about C₂₅H₂₄N₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13091-23-1
4-chloro-3-nitropyridine

: 701213-67-4
C₂₅H₂₄N₆O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / -20 °C

2: aluminum (III) chloride; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride

3: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

4: copper; potassium carbonate / 160 °C / Microwave irradiation

With aluminum (III) chloride; copper; potassium carbonate; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; N,N-dimethyl-formamide; 1: |Bartoli Indole Synthesis;
DOI:10.1016/j.bmcl.2012.10.120

Reference yield:

: 357263-48-0
7-chloro-1H-pyrrolo[3,2-b]pyridine

: 701213-67-4
C₂₅H₂₄N₆O₃

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride

2: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

3: copper; potassium carbonate / 160 °C / Microwave irradiation

With aluminum (III) chloride; copper; potassium carbonate; 1-ethyl-3-methyl-1H-imidazol-3-ium chloride; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.10.120

Reference yield:

: 791053-66-2
(7-chloro-1H-pyrrolo[3,2-b]pyridin-3-yl)-oxo-acetic acid

: 701213-67-4
C₂₅H₂₄N₆O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: copper; potassium carbonate / 160 °C / Microwave irradiation

With copper; potassium carbonate; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.10.120