Essigsaeure-

Base Information

• Chemical Name: Essigsaeure-
• CAS No.: 36842-84-9
• Molecular Formula: C₁₀H₁₂ClNO
• Molecular Weight: 197.664

Synonyms:

Chemical Property of Essigsaeure-

Chemical Property:

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Technology Process of Essigsaeure-

There total 2 articles about Essigsaeure- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetyl chloride (75-36-5) + 2-ethoxy-3-phenyl-1,3,2-oxazaphospholidine (5679-72-1) → Essigsaeure- (36842-84-9)

Guidance literature:

Reference yield:

→ Essigsaeure- (36842-84-9)

Guidance literature:

1,3,2-Oxazaphospholan (I), Acetylchlorid;

DOI:10.1007/BF00924420

Reference yield: 65.0%

Essigsaeure- (36842-84-9) + lithium triphenylstannide (4167-90-2) → (C6H5)3SnCH2CH2N(C6H5)COCH3 (42428-61-5)

Guidance literature:

In tetrahydrofuran; 25 °C for 18 h, heated at reflux for 2 h;;

DOI:10.1021/jo00965a005

upstream raw materials:

acetyl chloride

2-ethoxy-3-phenyl-1,3,2-oxazaphospholidine

Downstream raw materials:

(C₆H₅)3SnCH₂CH₂N(C₆H₅)COCH₃

(C₆H₅)3SnCH₂CH₂NHC₆H₅

{(C₆H₅)3SnCH₂CH₂NH₂C₆H₅}⁽¹⁺⁾*Br^(1-)={(C₆H₅)3SnCH₂CH₂NH₂C₆H₅}Br

{(C₆H₅)Cl₂SnCH₂CH₂NH₂C₆H₅}⁽¹⁺⁾*Cl^(1-)={(C₆H₅)Cl₂SnCH₂CH₂NH₂C₆H₅}Cl

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