3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, mono[(1-oxopropoxy)methyl] ester, (R)-

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, mono[(1-oxopropoxy)methyl] ester, (R)-
CAS No.:138279-22-8
Molecular Formula:C₂₁H₂₄N₂O₉
Molecular Weight:448.43
Hs Code.:
Mol file:138279-22-8.mol

Synonyms:

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, mono[(1-oxopropoxy)methyl] ester, (R)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, mono[(1-oxopropoxy)methyl] ester, (R)-

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Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, mono[(1-oxopropoxy)methyl] ester, (R)-

There total 5 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, mono[(1-oxopropoxy)methyl] ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 138279-15-9
bis(propionyloxymethyl) 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

: 138279-22-8,138693-53-5
1-Methoxymethyl-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid monopropionyloxymethyl ester

Guidance literature:: In di-isopropyl ether; water; at 0 - 5 ℃; for 8h; lipase B;
DOI:10.1016/S0040-4039(00)93560-3

Reference yield:

: 123973-70-6
1,4-dihydro-2,6-dimethyl-1-methoxymethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylic acid

: 138279-22-8,138693-53-5
1-Methoxymethyl-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid monopropionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylformamide

2: 71 percent / diisopropyl ether; H₂O / 8 h / 0 - 5 °C / lipase B

With sodium hydride; In di-isopropyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)93560-3

Reference yield:

: 123973-70-6
1,4-dihydro-2,6-dimethyl-1-methoxymethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylic acid

: 138279-22-8,138693-53-5
1-Methoxymethyl-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid monopropionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylformamide

2: diisopropyl ether; H₂O / 10 h / 25 °C / lipase P

With sodium hydride; In di-isopropyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)93560-3