3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, methyl (1-oxopropoxy)methyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, methyl (1-oxopropoxy)methyl ester
CAS No.:138299-12-4
Molecular Formula:C₂₂H₂₆N₂O₉
Molecular Weight:462.456
Hs Code.:
Mol file:138299-12-4.mol

Synonyms:

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, methyl (1-oxopropoxy)methyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, methyl (1-oxopropoxy)methyl ester

There total 3 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-, methyl (1-oxopropoxy)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123973-70-6
1,4-dihydro-2,6-dimethyl-1-methoxymethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylic acid

: 138299-12-4
1-Methoxymethyl-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-methyl ester 5-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dimethylformamide

2: 71 percent / diisopropyl ether; H₂O / 8 h / 0 - 5 °C / lipase B

3: CH₂Cl₂

With sodium hydride; In dichloromethane; di-isopropyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)93560-3

Reference yield:

: 138279-15-9
bis(propionyloxymethyl) 1,4-dihydro-1-(methoxymethyl)-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

: 138299-12-4
1-Methoxymethyl-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-methyl ester 5-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / diisopropyl ether; H₂O / 8 h / 0 - 5 °C / lipase B

2: CH₂Cl₂

In dichloromethane; di-isopropyl ether; water;
DOI:10.1016/S0040-4039(00)93560-3