3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(trifluoromethyl)phenyl]-, (2,2-dimethyl-1-oxopropoxy)methyl methyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(trifluoromethyl)phenyl]-, (2,2-dimethyl-1-oxopropoxy)methyl methyl ester
CAS No.:138279-27-3
Molecular Formula:C₂₃H₂₆F₃NO₆
Molecular Weight:469.458
Hs Code.:
Mol file:138279-27-3.mol

3,5-Pyridinedicarboxylic acid,
1,4-dihydro-2,6-dimethyl-4-[2-(trifluoromethyl)phenyl]-,
(2,2-dimethyl-1-oxopropoxy)methyl methyl ester

Synonyms:

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(trifluoromethyl)phenyl]-, (2,2-dimethyl-1-oxopropoxy)methyl methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(trifluoromethyl)phenyl]-, (2,2-dimethyl-1-oxopropoxy)methyl methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(trifluoromethyl)phenyl]-, (2,2-dimethyl-1-oxopropoxy)methyl methyl ester

There total 5 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(trifluoromethyl)phenyl]-, (2,2-dimethyl-1-oxopropoxy)methyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138279-24-0
1-Methoxymethyl-2,6-dimethyl-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2,2-dimethyl-propionyloxymethyl) ester 5-methyl ester

: 138279-27-3
2,6-Dimethyl-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2,2-dimethyl-propionyloxymethyl) ester 5-methyl ester

Guidance literature:: With hydrogenchloride; In acetone;
DOI:10.1016/S0040-4039(00)93560-3

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 138279-27-3
2,6-Dimethyl-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2,2-dimethyl-propionyloxymethyl) ester 5-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / dimethylformamide

2: 83 percent / diisopropyl ether; H₂O / 7 h / 25 °C / lipase B

3: CH₂Cl₂

4: dil. HCl / acetone

With hydrogenchloride; sodium hydride; In dichloromethane; di-isopropyl ether; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(00)93560-3

Reference yield:

: 141600-82-0
1-Methoxymethyl-2,6-dimethyl-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid

: 138279-27-3
2,6-Dimethyl-4-(2-trifluoromethyl-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2,2-dimethyl-propionyloxymethyl) ester 5-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / dimethylformamide

2: 83 percent / diisopropyl ether; H₂O / 7 h / 25 °C / lipase B

3: CH₂Cl₂

4: dil. HCl / acetone

With hydrogenchloride; sodium hydride; In dichloromethane; di-isopropyl ether; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4039(00)93560-3