Technology Process of (8S,9S)-8-methoxy-9-methylheptacosanal
There total 1 articles about (8S,9S)-8-methoxy-9-methylheptacosanal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium bicarbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 87 percent / lithium hexamethyldisilazide / tetrahydrofuran / 16 h / 20 °C
2: 100 percent / hydrogen / palladium on charcoal / ethanol
3: 95 percent / potassium hydroxide / methanol; tetrahydrofuran / 3 h / 40 °C
4: 76 percent / N-bromosuccinimide; triphenylphosphine / CH2Cl2 / 1 h / 0 °C
5: 99 percent / potassium carbonate / acetone / 18 h / 20 - 40 °C
With
potassium hydroxide; N-Bromosuccinimide; hydrogen; potassium carbonate; triphenylphosphine; lithium hexamethyldisilazane;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetone;
1: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2007.01.007
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 87 percent / lithium hexamethyldisilazide / tetrahydrofuran / 16 h / 20 °C
2: 100 percent / hydrogen / palladium on charcoal / ethanol
3: 95 percent / potassium hydroxide / methanol; tetrahydrofuran / 3 h / 40 °C
4: 76 percent / N-bromosuccinimide; triphenylphosphine / CH2Cl2 / 1 h / 0 °C
5: 99 percent / potassium carbonate / acetone / 18 h / 20 - 40 °C
6: 91 percent / ammonium heptamolybdate(VI) tetrahydrate; aq. hydrogen peroxide / tetrahydrofuran; various solvent(s) / 1 h / 20 °C
With
potassium hydroxide; N-Bromosuccinimide; ammonium molybdate tetrahydrate; hydrogen; dihydrogen peroxide; potassium carbonate; triphenylphosphine; lithium hexamethyldisilazane;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetone;
1: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2007.01.007
